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6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)

Product Introduction

6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)- Basic information

Product Name:	6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)-
Synonyms:	6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)-;(S,E)-8-Methyl-5-(1-methylethyl)-6,8-nonadien-2-one;[S,6E,(+)]-5-Isopropyl-8-methyl-6,8-nonadien-2-one;8-Nonadien-2-one, 8-Methyl-5-(1-Methylethyl)-, (5S,6E)-;Solanone DISCONTINUED;(5S,6E)-8-Methyl-5-(1-Methylethyl)-6,8-Nonadien-2-One;D-Solanone
CAS:	1937-54-8
MF:	C13H22O
MW:	194.31
EINECS:
Product Categories:
Mol File:	1937-54-8.mol

6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)- Chemical Properties

alpha	D23 +13.6° (neat)
Boiling point	bp1 60°
density	d420 0.870
refractive index	nD20 1.4755
EPA Substance Registry System	6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)- (1937-54-8)

Safety Information

MSDS Information

6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)- Usage And Synthesis

Uses	Solanone is use as a flavoring agent in cigarettes. The compound can be optioned from Nicotiana glutinosa L. leaves.
Purification Methods	Purify solanone by high vacuum distillation and store it in sealed ampules [Kohda & Sato J Chem Soc, Chem Commun 951 1981]. It has UV (hexane) at max 230nm ( 11,800). The semicarbazone crystallises from aqueous EtOH or toluene with m 160.5-161.5o. [Johnson et al. J Org Chem 30 2918 1965.]

6,8-Nonadien-2-one, 8-methyl-5-(1-methylethyl)-, (5S,6E)- Preparation Products And Raw materials

Raw materials

(3R)-6-methyl-3-propan-2-yl-7-oxabicyclo[4.1.0]heptane-->Hexanal, 2-(1-methylethyl)-5-oxo-, (2S)--->(+)-P-MENTH-1-ENE-->DIETHYL (2-METHYLALLYL)PHOSPHONATE 97-->2-BROMOPROPENE-->(+)-Dipentene

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